| Preparation of shuttle-like Sb2S3 nanorod-bundles via a solvothermal approach under alkaline condition | |
| Department | 固体润滑国家重点实验室 ; 先进润滑与防护材料研究发展中心 |
Zhang L(张玲); Chen L(陈磊) ; Wan HQ(万宏启); Zhou HD(周惠娣); Chen JM(陈建敏)
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| 2010 | |
| Source Publication | Cryst. Res. Technol.
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| ISSN | 0232-1300 |
| Volume | 45Issue:2Pages:178-182 |
| Abstract | Uniform shuttle-like Sb2S3 nanorod-bundles were synthesized via a polyvinylpyrrolidone (PVP) assisted solvothermal approach under alkaline condition, using antimony chloride (SbCl3) and thiourea (CH4N2S, Tu) as the starting materials in ethanol. The phase structure, composition and morphology of the product were characterized by means of X-ray diffraction (XRD), energy dispersive X-ray spectrometry (EDS), transmission electron microscopy (TEM), and high-resolution transmission electron microscopy (HRTEM). XRD and EDS results confirm that the synthesized Sb2S3 nanorod-bundles have an orthorhombic structure and an atomic ratio of 3:2 for S:Sb. TEM and HRTEM results show that the shuttle-like Sb2S3 bundles are composed of nanorods with a size distribution of 20-40 nm and growing along c-axis. Furthermore, experiments under different reaction conditions were carried out and the mechanism for the growth of nanorod-bundles was discussed. |
| Keyword | Nanostructure Semiconductor Crystal Growth |
| Subject Area | 材料科学与物理化学 |
| Funding Organization | the “973” Program of China (Grant No. 2007CB607601);the Innovative Group Fund of National Natural Science Foundation of China (NNSFC, Grant No. 50421502) |
| Indexed By | SCI |
| Language | 英语 |
| Funding Project | 磨损和表面工程组 |
| Citation statistics | |
| Document Type | 期刊论文 |
| Identifier | http://ir.licp.cn/handle/362003/981 |
| Collection | 固体润滑国家重点实验室（LSL） 中国科学院材料磨损与防护重点实验室/先进润滑与防护材料研究发展中心 |
| Corresponding Author | Chen JM(陈建敏) |
| Recommended Citation GB/T 7714 | Zhang L,Chen L,Wan HQ,et al. Preparation of shuttle-like Sb2S3 nanorod-bundles via a solvothermal approach under alkaline condition[J]. Cryst. Res. Technol.,2010,45(2):178-182. |
| APA | 张玲,陈磊,万宏启,周惠娣,&陈建敏.(2010).Preparation of shuttle-like Sb2S3 nanorod-bundles via a solvothermal approach under alkaline condition.Cryst. Res. Technol.,45(2),178-182. |
| MLA | 张玲,et al."Preparation of shuttle-like Sb2S3 nanorod-bundles via a solvothermal approach under alkaline condition".Cryst. Res. Technol. 45.2(2010):178-182. |
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| 2010178-182.pdf（439KB） | 开放获取 | License | View Application Full Text | |||
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