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N,N’-双-三唑甲基-[2,2]的合成及晶体结构
Department非现建制
高志昌; 赵建生; 金钟声; 刘永盛; 胡宁海
1988
Source Publication结构化学
ISSN0254-5861
Volume7Issue:4Pages:315-321
Abstract标题化合物由N,N′-双-甲氧基甲基[2,2]和1H1,2,4-三唑在无溶剂的情况下反应得到。它的单晶X射线分析表明晶体属正交晶系, 空间群为Pca21, 晶胞参数:a=9.986(3)、b=12.932(6)、c=17.135(6)Å, z=4。结构用直接法解出, 经块矩阵最小二乘法修正, 最后的R=0.042。该冠醚环的C—C、N—C与O—C的平均键长分别为1.50(1)、1.40(1)、1.43(1)Å, 三唑(a)与(b)的五个键长的平均值皆为1.33(1)Å。
Subject Area物理化学
Language中文
Document Type期刊论文
Identifierhttp://ir.licp.cn/handle/362003/6156
Collection非现建制
Recommended Citation
GB/T 7714
高志昌,赵建生,金钟声,等. N,N’-双-三唑甲基-[2,2]的合成及晶体结构[J]. 结构化学,1988,7(4):315-321.
APA 高志昌,赵建生,金钟声,刘永盛,&胡宁海.(1988).N,N’-双-三唑甲基-[2,2]的合成及晶体结构.结构化学,7(4),315-321.
MLA 高志昌,et al."N,N’-双-三唑甲基-[2,2]的合成及晶体结构".结构化学 7.4(1988):315-321.
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