| Fabrication of TiN nanorods by electrospinning and their electrochemical properties | |
| Department | 固体润滑国家重点实验室 ; 先进润滑与防护材料研究发展中心 |
Sun DF(孙东飞); Lang JW(郎俊伟); Yan XB(阎兴斌) ; Hu LT(胡丽天); Xue QJ(薛群基)
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| 2011 | |
| Source Publication | Journal of Solid State Chemistry
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| ISSN | 0022-4596 |
| Volume | 184Pages:1333-1338 |
| Abstract | TiN nanorods were synthesized using electrospinning technique followed by thermolysis in different atmospheres. A dimethyl formamide–ethanol solution of poly-(vinyl pyrrolidone) and Ti (IV)-isoprop- oxide was used as the electrospinning precursor solution and as-spun nanofibers were calcined at 500 1C in air to generate TiO2 nanofibers. Subsequently, a conversion from TiO2 nanofibers to TiN nanorods was employed by the nitridation treatment at 600 1400 1C in ammonia atmosphere. A typical characteristic of the final products was that the pristine nanofibers were cut into nanorods. The conversion from TiO2 to TiN was realized when the nitridation temperature was above 800 1C. As-prepared nanorods were composed of TiN nano-crystallites and the average crystallite size gradually increased with the increase of the nitridation temperature. Electrochemical properties of TiN nanorods showed strong dependence on the nitridation temperature. The maximum value of the specific capacitance was obtained from the TiN nanorods prepared at 800 C. |
| Keyword | Tin Nanorod Electrospinning Electrochemical Property Capacitance |
| Subject Area | 材料科学与物理化学 |
| Funding Organization | the Top Hundred Talents Program of Chinese Academy of Sciences;the National Basic Research 973 Program of China (2011CB706603);the National Nature Science Foundation of China (51005225) |
| Indexed By | SCI |
| Language | 英语 |
| Funding Project | 低维材料摩擦学组 ; 特种油脂和密封材料组 |
| Citation statistics | |
| Document Type | 期刊论文 |
| Identifier | http://ir.licp.cn/handle/362003/3253 |
| Collection | 固体润滑国家重点实验室（LSL） 中国科学院材料磨损与防护重点实验室/先进润滑与防护材料研究发展中心 |
| Corresponding Author | Yan XB(阎兴斌) |
| Recommended Citation GB/T 7714 | Sun DF,Lang JW,Yan XB,et al. Fabrication of TiN nanorods by electrospinning and their electrochemical properties[J]. Journal of Solid State Chemistry,2011,184:1333-1338. |
| APA | 孙东飞,郎俊伟,阎兴斌,胡丽天,&薛群基.(2011).Fabrication of TiN nanorods by electrospinning and their electrochemical properties.Journal of Solid State Chemistry,184,1333-1338. |
| MLA | 孙东飞,et al."Fabrication of TiN nanorods by electrospinning and their electrochemical properties".Journal of Solid State Chemistry 184(2011):1333-1338. |
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| 20111333-1338.PDF（1411KB） | 开放获取 | License | View Application Full Text | |||
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