Chloromethylation research of LX-1180 macroporous adsorption resin in ultrasonic environment | |
Department | 甘肃省天然药物重点实验室 |
Chen ZB(陈振斌); Kang L(康磊); Di DL(邸多隆); Dong F(董方); Yu H(余辉) | |
2011 | |
Source Publication | Advanced Materials Research |
ISSN | 1022-6680 |
Volume | 233-235Pages:2893-2897 |
Abstract | This work performed the chloromethylation study of LX1180 in an ultrasonic environment, and presented a novel method to realize high chloromethylation degree for high crosslinking MARs. During this process, Monochloromethyl ether and anhydrous zinc chloride was adopted as chloromethylation reagent and catalyst respectively, the influences of conditions on the chloromethylation degree were investigated and optimized systemically. The sample prepared under the optimization conditions possessed the chloromethylation degree of 2.87 mmol/g. |
Keyword | Ultrasonic Catalysis Chloromethylation Macroporous Adsorption Resin |
Subject Area | 分析化学与药物化学 |
Indexed By | EI |
Language | 英语 |
Funding Project | 药物工艺标准研究组 |
Document Type | 期刊论文 |
Identifier | http://ir.licp.cn/handle/362003/2233 |
Collection | 中科院西北特色植物资源化学重点实验室/甘肃省天然药物重点实验室 |
Corresponding Author | Di DL(邸多隆) |
Recommended Citation GB/T 7714 | Chen ZB,Kang L,Di DL,et al. Chloromethylation research of LX-1180 macroporous adsorption resin in ultrasonic environment[J]. Advanced Materials Research,2011,233-235:2893-2897. |
APA | 陈振斌,康磊,邸多隆,董方,&余辉.(2011).Chloromethylation research of LX-1180 macroporous adsorption resin in ultrasonic environment.Advanced Materials Research,233-235,2893-2897. |
MLA | 陈振斌,et al."Chloromethylation research of LX-1180 macroporous adsorption resin in ultrasonic environment".Advanced Materials Research 233-235(2011):2893-2897. |
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