Chloromethylation research of LX-1180 macroporous adsorption resin in ultrasonic environment
Department甘肃省天然药物重点实验室
Chen ZB(陈振斌); Kang L(康磊); Di DL(邸多隆); Dong F(董方); Yu H(余辉)
2011
Source PublicationAdvanced Materials Research
ISSN1022-6680
Volume233-235Pages:2893-2897
AbstractThis work performed the chloromethylation study of LX1180 in an ultrasonic environment, and presented a novel method to realize high chloromethylation degree for high crosslinking MARs. During this process, Monochloromethyl ether and anhydrous zinc chloride was adopted as chloromethylation reagent and catalyst respectively, the influences of conditions on the chloromethylation degree were investigated and optimized systemically. The sample prepared under the optimization conditions possessed the chloromethylation degree of 2.87 mmol/g.
KeywordUltrasonic Catalysis Chloromethylation Macroporous Adsorption Resin
Subject Area分析化学与药物化学
Indexed ByEI
Language英语
Funding Project药物工艺标准研究组
Document Type期刊论文
Identifierhttp://ir.licp.cn/handle/362003/2233
Collection中科院西北特色植物资源化学重点实验室/甘肃省天然药物重点实验室
Corresponding AuthorDi DL(邸多隆)
Recommended Citation
GB/T 7714
Chen ZB,Kang L,Di DL,et al. Chloromethylation research of LX-1180 macroporous adsorption resin in ultrasonic environment[J]. Advanced Materials Research,2011,233-235:2893-2897.
APA 陈振斌,康磊,邸多隆,董方,&余辉.(2011).Chloromethylation research of LX-1180 macroporous adsorption resin in ultrasonic environment.Advanced Materials Research,233-235,2893-2897.
MLA 陈振斌,et al."Chloromethylation research of LX-1180 macroporous adsorption resin in ultrasonic environment".Advanced Materials Research 233-235(2011):2893-2897.
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