Ionic Liquid-Assisted Hydrothermal Method Synthesis of Flower-Like MoS2 and Their Electrochemical Performances | |
Department | 固体润滑国家重点实验室 |
Li, Maohua1,2; Yang, Bo2; Hao JY(郝俊英)3; Lu, Yi1,2; Long, Zerong2; Liu, Yumei1 | |
2016 | |
Source Publication | Journal of Nanoscience and Nanotechnology |
ISSN | 1533-4880 |
Volume | 16Issue:6Pages:6238-6245 |
Abstract | Molybdenum disulfide (MoS2) was prepared successfully via hydrothermal reaction at 200 °C in water/ethanol (1:1) solvent system using the ammonium molybdate and sodium thiosulfate as the molybdenum sources and sulfur sources, 1-butyl-3-methylimidazolium chloride salt [BMIM][Cl] as the additive agent. The scanning electron microscopy (SEM) and transmission electron microscopy (TEM) were used to examine the morphology and structure of flower-like products. X-ray photoelectron spectroscopy (XPS) and Raman spectroscopy spectrum analysis results show that the asprepared product is a pure phase of MoS2. The prepared products are used as electrode materials for Li-ion batteries and showed excellent cycle stability and high Coulombic efficiency at a current density of 200 mA·g−1 in the voltage range of 0.01∼3.00 V (vs. Li/Li+). In addition, this paper also examined the influence of the reaction time and the amount of template agent on morphology, and discussed the reaction mechanism of the formation of flower-like morphology. |
Keyword | Hydrothermal Reaction Ionic Liquids Flower-like Morphology Mos2 Electrochemistry |
Subject Area | 材料科学与物理化学 |
DOI | 10.1166/jnn.2016.10898 |
Funding Organization | the National Natural Science Foundation of China (No. 51375471);the major project of Xinjiang Bureau of Quality and Technical Supervision (No. 2013-01);the science and technology project of State Quality Inspection Administration (2013QK086) |
Indexed By | SCI |
If | 1.483 |
Language | 英语 |
Funding Project | 空间润滑材料组 |
compositor | 第三作者单位 |
Citation statistics | |
Document Type | 期刊论文 |
Identifier | http://ir.licp.cn/handle/362003/20992 |
Collection | 固体润滑国家重点实验室(LSL) |
Corresponding Author | Lu, Yi |
Affiliation | 1.Xinjiang Univ, Coll Chem & Chem Engn, Urumqi 830046, Peoples R China 2.Xinjiang Supervis & Inspect Inst Prod Qual, Urumqi 830011, Peoples R China 3.Chinese Acad Sci, State Key Lab Solid Lubricat, Lanzhou 730000, Peoples R China |
Recommended Citation GB/T 7714 | Li, Maohua,Yang, Bo,Hao JY,et al. Ionic Liquid-Assisted Hydrothermal Method Synthesis of Flower-Like MoS2 and Their Electrochemical Performances[J]. Journal of Nanoscience and Nanotechnology,2016,16(6):6238-6245. |
APA | Li, Maohua,Yang, Bo,Hao JY,Lu, Yi,Long, Zerong,&Liu, Yumei.(2016).Ionic Liquid-Assisted Hydrothermal Method Synthesis of Flower-Like MoS2 and Their Electrochemical Performances.Journal of Nanoscience and Nanotechnology,16(6),6238-6245. |
MLA | Li, Maohua,et al."Ionic Liquid-Assisted Hydrothermal Method Synthesis of Flower-Like MoS2 and Their Electrochemical Performances".Journal of Nanoscience and Nanotechnology 16.6(2016):6238-6245. |
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