| Green Synthesis of N-Sulfonylimine in Solvent-Free Condition with Heteropoly Acid as Catalyst | |
| Department | OSSO国家重点实验室 |
Wang DS(王德胜)1,2; Yan L(闫亮)1 ; Wang XL(王晓来)1
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| 2012 | |
| Source Publication | Asian Journal of Chemistry
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| ISSN | 0970-7077 |
| Volume | 24Issue:6Pages:2724-2726 |
| Abstract | A new method for the synthesis of N-sulfonylimine directly from benzaldehyde and p-methylphenyl sulphonylamine with Keggin type heteropoly acid as reusable catalyst in solvent-less condition had been investigated. H3PW12 is found to be the most efficient activity and affording N-sulfonylimine in the yield of 86 %. H3PW12 catalyst reserved its' activity and the yield decreased slightly after running for 5 times. The facial catalytic separation and the reusability of the H3PW12 may hopefully contribute to the development of green chemistry and the environmental benign strategy for the synthesis of N-sulfonylimine. |
| Keyword | Heteropoly Acid Condensation Synthetic Method Sulfonamide Solvent Free |
| Subject Area | 物理化学与绿色催化 |
| Indexed By | SCI |
| If | 0.253 |
| Language | 英语 |
| Funding Project | 多相选择氧化课题组 |
| compositor | 第一作者单位 |
| Citation statistics | |
| Document Type | 期刊论文 |
| Identifier | http://ir.licp.cn/handle/362003/19449 |
| Collection | 羰基合成与选择氧化国家重点实验室（OSSO） |
| Affiliation | 1.Chinese Acad Sci, Lanzhou Inst Chem Phys, State Key Lab Oxo Synth & Select Oxidat, Lanzhou 730000, Peoples R China 2.Chinese Acad Sci, Grad Sch, Beijing 100000, Peoples R China |
| Recommended Citation GB/T 7714 | Wang DS,Yan L,Wang XL. Green Synthesis of N-Sulfonylimine in Solvent-Free Condition with Heteropoly Acid as Catalyst[J]. Asian Journal of Chemistry,2012,24(6):2724-2726. |
| APA | Wang DS,Yan L,&Wang XL.(2012).Green Synthesis of N-Sulfonylimine in Solvent-Free Condition with Heteropoly Acid as Catalyst.Asian Journal of Chemistry,24(6),2724-2726. |
| MLA | Wang DS,et al."Green Synthesis of N-Sulfonylimine in Solvent-Free Condition with Heteropoly Acid as Catalyst".Asian Journal of Chemistry 24.6(2012):2724-2726. |
| Files in This Item: | ||||||
| File Name/Size | DocType | Version | Access | License | ||
| LZ01028534.pdf（2757KB） | 期刊论文 | 作者接受稿 | 开放获取 | CC BY-NC-SA | View Application Full Text | |
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