| Preparation and evaluation of a novel cellulose tris(N-3,5-dimethylphenylcarbamate) chiral stationary phase | |
| Department | 甘肃省天然药物重点实验室 |
Ge J(葛晋); Zhao L(赵亮) ; Shi YP(师彦平)
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| 2008 | |
| Source Publication | Chinese Journal of Chemistry
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| ISSN | 1001-604X |
| Volume | 26Issue:1Pages:139-142 |
| Abstract | A novel cellulose tris(N-3,5-dimethylphenylcarbamate) (CDMPC) chiral stationary phase (CSP) was prepared by coating CDMPC on TiO2/SiO2, which was prepared by coating titania nanoparticles on silica through a self-assemble technique. At first, 2-hydroxyl-phenyl acetonitrile and α-phenylethanol were separated on this new CSP to evaluate the chiral separation ability. Then, two pesticides, matalaxyl and diclofop-methyl were separated. The influence of the mobile phase composition on the enantioselectivity was discussed, and the repeatability and stability of the CSP were studied too. |
| Keyword | Chiral Stationary Phase Tio2/sio2 Cellulose Tris(N-3 5-dimethylphenylcarbamate) |
| Subject Area | 分析化学与药物化学 |
| Funding Organization | the National Natural Science Foundation of China (Nos. 20375045;20475057;20675085);the Program of the Light in China's Western Region (2003);the Province Natural Science Foundation of Gansu (No. 3ZS041-A25-23) |
| Indexed By | SCI |
| Language | 英语 |
| Funding Project | 药物化学成分研究组 ; 药物手性分离研究组 |
| Citation statistics | |
| Document Type | 期刊论文 |
| Identifier | http://ir.licp.cn/handle/362003/1377 |
| Collection | 中科院西北特色植物资源化学重点实验室/甘肃省天然药物重点实验室 |
| Corresponding Author | Shi YP(师彦平) |
| Recommended Citation GB/T 7714 | Ge J,Zhao L,Shi YP. Preparation and evaluation of a novel cellulose tris(N-3,5-dimethylphenylcarbamate) chiral stationary phase[J]. Chinese Journal of Chemistry,2008,26(1):139-142. |
| APA | 葛晋,赵亮,&师彦平.(2008).Preparation and evaluation of a novel cellulose tris(N-3,5-dimethylphenylcarbamate) chiral stationary phase.Chinese Journal of Chemistry,26(1),139-142. |
| MLA | 葛晋,et al."Preparation and evaluation of a novel cellulose tris(N-3,5-dimethylphenylcarbamate) chiral stationary phase".Chinese Journal of Chemistry 26.1(2008):139-142. |
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